Editorial Type:
Article Category: Clinical Research
 | 
Online Publication Date: 01 Mar 2012

Clinical Evaluation of a Low-shrinkage Composite in Posterior Restorations: One-Year Results

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Page Range: 117 – 129
DOI: 10.2341/11-179-C
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SUMMARY

Objectives

The aim of this study was to compare the one-year clinical performance of three restorative systems, which included a novel low-shrinkage composite and two bonding strategies.

Materials and Methods

Twenty-five patients received three Class I (occlusal) or Class II restorations performed with one of three restorative systems: Filtek Silorane Restorative System (FS); Adper Scotchbond 1 XT, a two-step etch-and-rinse adhesive, with Filtek Z250 (XT); and Adper Scotchbond SE, a two-step self-etch adhesive, with Filtek Z250 (SE). All materials were applied following the manufacturer's instructions. Two independent observers evaluated the restorations at baseline, after six months, and after one year, according to the United States Public Health System modified criteria. The Kruskal-Wallis test and the Mann-Whitney U-test were computed to compare the behavior of the restorative systems; Friedman and Wilcoxon tests were used to analyze the intrasystem data (α=0.05).

Results

All restorations were evaluated at one year. FS and XT performed statistically similarly at one year, but marginal staining for SE was statistically worse. Intrasystem comparisons between baseline and one year also showed deterioration of marginal staining for SE, while a deterioration of the marginal adaptation was recorded for both SE and FS. XT was the only system for which there was no statistical change of the parameters measured in this study.

Conclusions

Both restorative systems using self-etch adhesives showed a tendency to degradation of marginal adaptation after one year of clinical use, compared to baseline values. Although the clinical performance of FS was deemed acceptable after one year, this study did not find any advantage of the silorane-based composite over the methacrylate-based composite. The low-shrinkage associated with FS may not be a determinant factor for clinical success.

INTRODUCTION

The improvements in dental adhesives and resin composites, along with a minimally invasive approach to caries treatment, have made these restorative materials very popular for direct posterior restorations. Nevertheless, the longevity of these restorations is still affected by the consequences of their polymerization shrinkage. The volumetric reduction due to polymerization generates stress within the material, at the adhesive interface, and in the tooth structure.1 The physical mismatch between the shrinkage-prone restorative material and the stiffer tooth structure may result in microleakage, marginal staining, gap formation, postoperative sensitivity, and enamel microcracks or cusp deflection.2,3

Filtek Silorane, introduced in 2007, is the first commercially available resin composite not based on bisphenol A diglycidyl methacrylate or urethane dimethacrylate, the dimethacrylate monomers most commonly used.4 This novel silorane-based resin takes its name from the combination of its chemical blocks, siloxanes and oxiranes. The silorane molecule has a siloxane core with four attached oxirane rings that open upon polymerization to bond to other monomers.5,6 This mechanism implies a slight reduction of the initial distance between monomers, which results in a volumetric shrinkage of less than 1%, which might generate less stress on the adhesive interface.5,7,8 This characteristic has been validated by other in vitro studies,9,10 in which the silorane-based resin resulted in a significantly lower cusp deflection when applied to MOD preparations, in comparison to methacrylate-based resins. Moreover, the silorane-based resin has been shown to have adequate physical and mechanical properties, which make it suitable for clinical application.6,11

The specific chemistry and curing mechanism of the silorane-based resin composite required the development of a dedicated adhesive by the respective manufacturer. In the case of Filtek Silorane, a two-step self-etch adhesive was developed. This adhesive is composed of a self-etch primer and a hydrophobic bonding resin.12,13 Self-etch adhesives have become increasingly popular as they are more user-friendly, less technique-sensitive, and may reduce postoperative sensitivity14,15 compared to etch-and-rinse adhesives. However, the adhesion to enamel achieved by etch-and-rinse adhesives is still considered the “gold standard”14,16,17 as a result of the deep etching pattern created by the low pH of phosphoric acid. Therefore, the performance of self-etch adhesives on enamel may depend on their aggressiveness. “Strong” self-etch adhesives result in a more stable and satisfactory enamel bond than do “mild” self-etch adhesives, especially on ground, aprismatic enamel.1820 In fact, selective etching of enamel margins with phosphoric acid has been recommended2123 in clinical situations prior to applying “mild” self-etch adhesives.

Clinical trials are the ultimate test with which to measure the clinical effectiveness and durability of adhesives and resin composites.24 This is of paramount relevance, as there is no clinical evidence to back the deleterious effect of polymerization stress on restoration longevity.25 Accordingly, the aim of this study was to compare the one-year clinical performance of three restorative systems in posterior restorations: the low-shrinkage silorane-based resin composite with its proprietary self-etch adhesive and a widely studied methacrylate-based resin composite, Filtek Z250, used with either a two-step etch-and-rinse adhesive or with a two-step self-etch adhesive. The null hypothesis was that there would be no differences in clinical performance for the three restorative systems after one year.

MATERIALS AND METHODS

Before participating in the study, subjects signed a written informed consent. Both the consent and this research protocol had previously been reviewed and approved by the Ethics Committee of the Rey Juan Carlos University.

All patients, with ages ranging from 18 to 60 years (average 29.8 years), required at least three Class I (occlusal) and/or Class II restorations (Table 1). The dental health status of patients was normal in all other respects. Specific exclusion criteria were as follows:

Table 1:  Number of Restorations by Location (Tooth) and Number of Surfaces for Each Restorative System
Table 1: 
  • Fewer than 20 teeth;

  • History of existing tooth sensitivity;

  • Periodontal disease;

  • Extremely poor oral hygiene;

  • Bruxism;

  • Known allergy to resin-based materials or other materials used in this study;

  • Pregnancy or breast-feeding; or

  • Chronic use of anti-inflammatory, analgesic, and psychotropic drugs.

Further, excluding criteria for the teeth to be restored were as follows:

  • Nonvital teeth;

  • Abutment teeth for fixed or removable prostheses; and

  • Teeth without a normal occlusal relationship with natural dentition or without at least one adjacent tooth contact.

Bitewing radiographs of the teeth to be restored were taken preoperatively, unless the patient had radiographs taken within the previous year. There was an even distribution of the restorations that replaced existing restorations with clinical or radiographic signs of recurrent caries or esthetic failures and restorations that were performed to treat primary caries lesions.

All operative procedures were performed by the same operator (B.B.). Restorations were placed under local anesthesia with rubber dam isolation. The cavity design was restricted to eliminate carious tissues from primary caries lesions or to remove the restorative material and carious tissues when existing restorations were replaced. Cavities were prepared using diamond burs (Komet-Brasseler, Lemgo, Germany) with no intentional bevels on enamel cavo-surface margins. In deep cavities, dentin was covered with a resin-modified glass ionomer cement (Vitrebond, 3M ESPE, St Paul, MN, USA). An appropriate matrix system (Palodent, Dentsply, Konstanz, Germany) and wooden wedges were applied to the cervical margins of proximal preparations.

The restorative systems evaluated in this study were the Filtek Silorane Restorative System, Adper Scotchbond 1 XT + Filtek Z250, and Adper Scotchbond SE + Filtek Z250 (Table 2).

Table 2:  Materials Used in the Study (3M ESPE, St Paul, MN, USA)
Table 2: 

Initially, the three restorative systems were randomly assigned to each of the three teeth for which restorative treatment was needed, regardless of the characteristics of the tooth and restoration class. However, interference in the randomization procedure within patients was eventually performed in order to equally distribute materials into some important variables, such as tooth type and position, restoration class, and restoration size, in such a way that the influence of those factors was minimized.26 All adhesive systems were applied according to the manufacturer‘s instructions (Table 2). Resin composites were placed in 2-mm increments. Each increment was light-cured for 20 seconds using a LED Demetron I polymerization unit (Kerr, Orange, CA, USA) with a minimum light output of 550 mW/cm2.

After polymerization, coarse finishing was accomplished with carbide burs under water cooling and, if needed, with a #12 blade and aluminum-oxide disks (Sof-Lex, 3M ESPE). Final finishing of the occlusal surface was accomplished with polishing points (Enhance and PoGo, Dentsply).

Clinical Evaluation

All restorations were evaluated after one week (baseline), six months, and one year for the following parameters: color match, retention, marginal adaptation, anatomic form, surface roughness, marginal staining, sensitivity, and secondary caries (Table 3). Pre- and postoperative sensitivity was determined with a dental syringe placed 2 cm from the tooth surface. Two clinicians (L.C. and E.C.) evaluated the restorations blindly at each recall using the modified United States Public Health Service (USPHS) criteria as adapted by Wilson and others27 (Table 3). When disagreements arose during evaluations, the examiners had to reach a consensus. To help with the evaluation of marginal discoloration, intraoral color photographs were collected at baseline and at the recall appointments. Clinical photographs consisted of digital images at 1.3× magnification taken with a Nikon D80 camera with a 105-mm Micro-Nikkor lens (Nikon USA, Melville, NY, USA).

Table 3:  Modified USPHS Criteria Used
Table 3: 

The statistical analyses were carried out with the SPSS 16.0 for Windows software (SPSS Inc, Chicago, IL, USA) using the nonparametric Kruskal-Wallis test and Mann-Whitney U-test to compare the behavior of the three restorative systems at baseline, six months, and one year. Friedman and Wilcoxon nonparametric tests were used to compare the data obtained for each restorative system at each evaluation period. The level of confidence was set at α = 0.05.

RESULTS

A total of 75 restorations were placed in 25 patients. The distribution of the restorations was similar between Class I (38) and Class II (37) cavities (Table 1). All patients attended the six-month and one-year recalls (100% recall rate). The results are summarized in Table 4.

Table 4:  Number of Evaluated Restorations in Each Criterion for Each Experimental Group
Table 4: 

Comparison of the Performance of the Three Restorative Systems at One Year

Adper Scotchbond SE + Filtek Z250 resulted in significantly worse marginal staining than did the other two restorative systems at one year (p=0.028). This deterioration had already been detected at the six-month recall appointment (p=0.013) (Figure 1).

Figure 1. . First molar. Occlusal restoration with Adper Scotchbond SE and Filtek Z250. Staining around this Class I restoration was observed at six-month and one-year evaluations, being rated Charlie (>50% of cavo-surface is affected). Furthermore, the one-year photograph shows that staining has progressed in depth across the adhesive interface. This stain also caused color changes in the resin composite close to the bonded walls. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 1. . First molar. Occlusal restoration with Adper Scotchbond SE and Filtek Z250. Staining around this Class I restoration was observed at six-month and one-year evaluations, being rated Charlie (>50% of cavo-surface is affected). Furthermore, the one-year photograph shows that staining has progressed in depth across the adhesive interface. This stain also caused color changes in the resin composite close to the bonded walls. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 1. . First molar. Occlusal restoration with Adper Scotchbond SE and Filtek Z250. Staining around this Class I restoration was observed at six-month and one-year evaluations, being rated Charlie (>50% of cavo-surface is affected). Furthermore, the one-year photograph shows that staining has progressed in depth across the adhesive interface. This stain also caused color changes in the resin composite close to the bonded walls. B, baseline; 6M, six-month recall; 1Y, one-year recall.
Figure 1.  First molar. Occlusal restoration with Adper Scotchbond SE and Filtek Z250. Staining around this Class I restoration was observed at six-month and one-year evaluations, being rated Charlie (>50% of cavo-surface is affected). Furthermore, the one-year photograph shows that staining has progressed in depth across the adhesive interface. This stain also caused color changes in the resin composite close to the bonded walls. B, baseline; 6M, six-month recall; 1Y, one-year recall.

Citation: Operative Dentistry 37, 2; 10.2341/11-179-C

All restorative systems resulted in a percentage of Alfa ratings above 90% at one year for the categories of retention and anatomical form. However, Alfa ratings for surface roughness, and in particular, marginal adaptation, decreased for all of the restorative systems, although this reduction did not result in statistical differences among them. Secondary caries was only detected in one tooth restored with Filtek Silorane, which had previously shown a fracture of the material at the six-month evaluation. Both findings had no statistical repercussions.

Baseline vs One-year Evaluation for Each Restorative System

Filtek Silorane Restorative System

Marginal adaptation was significantly worse at one year compared to baseline (p=0.005), as seven of 25 restorations were rated Bravo and one was rated Charlie. Additionally, surface roughness was statistically similar at baseline and after one year, but it was different at six months (p=0.02), as 28% of the restorations were rated Bravo at this recall. Filtek Silorane was the only system that rated Bravo in secondary caries and retention, Charlie in adaptation and anatomical form, and Delta in surface roughness. However, all of these ratings came from a single restoration and did not lead to any statistical significance. Only one restoration showed a true color modification over time, and two did not match adjacent tooth structure because of the yellowish and very opaque aspect of the Filtek Silorane resin composite.

Adper Scotchbond 1 XT + Filtek Z250

Marginal staining, surface roughness, and in particular marginal adaptation parameters resulted in worse rankings at one year (four restorations were rated Bravo), although there were no statistical differences (p>0.05). No Charlie ratings were assigned to this restorative system for any of the criteria. Postoperative sensitivity (slight discomfort associated with cold beverages) was found in one patient during the first week after the restoration was placed.

Adper Scotchbond SE + Filtek Z250

Marginal adaptation and marginal staining were significantly worse at one year compared to baseline. Adaptation deficiencies increased (p=0.002) in the last six months, as seven restorations rated Bravo and one was rated Charlie at one year. Marginal staining appeared during the first six months (p=0.014) and remained stable at the one-year recall, when eight restorations rated Bravo and one was rated Charlie. This restorative system was the only one that resulted in one Charlie rating for color match. Additionally, one patient experienced postoperative sensitivity after restoration placement, which disappeared gradually after a few days.

DISCUSSION

In this study, Filtek Silorane and the etch-and-rinse adhesive Adper Scotchbond 1 XT + Filtek Z250 resulted in statistically similar clinical parameters at one year. The other system formed by the self-etch adhesive Adper Scotchbond SE and Filtek Z250 resulted in increased marginal staining at one year. Thus, the first null hypothesis must be partially rejected.

Early marginal staining is usually a clinical sign that a restoration is prone to failure or that the adhesive interface undergoes degradation with time.28 Marginal discoloration may be caused by several factors, including the presence of excess filling materials, a deficient restoration around the margin, and the formation of gaps.29 However, the nature of the adhesive system is a determinant factor. The marginal staining associated with Adper Scotchbond SE + Filtek Z250 restorations must have been caused by the adhesive itself, since the other system using the same resin composite showed no alteration in this parameter. Adper Scotchbond SE is a strong self-etch system (pH=1).30 Although marginal discoloration has been associated with a poor etching ability of self-etch adhesives at the enamel margins,21,23,28 significant marginal staining and color changes have been reported for self-etch adhesives with a pH similar to that of Adper Scotchbond SE.28 Adper Scotchbond SE is a two-step self-etch adhesive in which water is separate from the adhesive solution to increase stability of the material.31 In fact, conventional methacrylate monomers undergo rapid hydrolysis under acidic aqueous conditions.31 Liquid A is a 2-hydroxyethyl methacrylate (HEMA)–water solution without etching capacity, and Liquid B is the solution containing the acidic monomers. The combination of acidic hydrophilic and hydrophobic monomers in the same solution (in this case, Liquid B) may cause a low degree of carbon double bond (C=C) conversion and increased permeability of adhesive interfaces. Other factors may be responsible for the marginal staining observed in the current study with SE. The change of color from pink to yellow that results from the adequate mix of Liquid A and Liquid B confirms that the acidic monomers have been activated (ionized). However, the activation of Liquid B into an etching agent, based on the superficial moisture provided by the 80% water in Liquid A, may result in an incomplete conversion of the acidic monomers. Their inclusion in a HEMA-rich and still-colored adhesive interface would enhance their susceptibility to hydrolytic degradation and, consequently, marginal staining.30,32 This mechanism was corroborated by the presence of the characteristic pink color of Liquid A in most of the stained margins around Adper Scotchbond SE + Filtek Z250 restorations (Figure 1).

A recent study32 has revealed high color instability after water immersion of a self-etch adhesive (One-Up Bond F, Tokuyama Dental Corporation, Tokyo, Japan), with a very similar color-change mechanism to that of Adper Scotchbond SE. Water sorption and discoloration of the adhesive interface may affect the color appearance of the restoration.32 This phenomenon is highly consistent with what evaluators found in the present study, as all the restorations with Adper Scotchbond SE + Filtek Z250 that rated Bravo or Charlie for color match presented a variable saturation of pink. Some of these restorations already had slight pink marginal staining at the baseline evaluation (Figure 1).

Regarding the comparisons between the baseline and one year for each restorative system, only Adper Scotchbond 1 XT + Filtek Z250 was statistically invariable for all of the parameters tested (Figure 2). Therefore, the second null hypothesis must also be partially rejected. The only system including an etch-and-rinse adhesive obtained the best clinical outcome, which is consistent with the results of previous clinical research.21,28 Moreover, in a literature review33 focused on marginal integrity, significantly better in vitro and in vivo enamel marginal adaptation were found with etch-and rinse adhesives compared to self-etch systems.

Figure 2. . First molar. Occlusal restoration with Adper Scotchbond 1 XT and Filtek Z250. This restoration preserved its original aspect after six months and one year. No signs of adhesive deterioration were found. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 2. . First molar. Occlusal restoration with Adper Scotchbond 1 XT and Filtek Z250. This restoration preserved its original aspect after six months and one year. No signs of adhesive deterioration were found. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 2. . First molar. Occlusal restoration with Adper Scotchbond 1 XT and Filtek Z250. This restoration preserved its original aspect after six months and one year. No signs of adhesive deterioration were found. B, baseline; 6M, six-month recall; 1Y, one-year recall.
Figure 2.  First molar. Occlusal restoration with Adper Scotchbond 1 XT and Filtek Z250. This restoration preserved its original aspect after six months and one year. No signs of adhesive deterioration were found. B, baseline; 6M, six-month recall; 1Y, one-year recall.

Citation: Operative Dentistry 37, 2; 10.2341/11-179-C

Restorations performed with Adper Scotchbond SE + Filtek Z250 exhibited a statistically lower number of Alfa ratings for marginal adaptation and marginal staining parameters at one year. Filtek Silorane also resulted in significantly worse marginal adaptation after one year. Marginal adaptation is influenced by many factors, such as the polymerization shrinkage of the composite resin or the adhesive system used.34 Both factors could influence the clinical results of this study, since restorative systems were made of different resin composites and adhesives.

Polymerization shrinkage of resin composites may be a potentially harmful factor for the clinical survival of direct restorations as a result of the transfer of stresses to the adhesive interface.35 Ideally, marginal adaptation, which depends on polymerization shrinkage and resulting stress, should be assessed at baseline because both shrinkage and resulting stress take place during the placement of the restoration. Other clinical factors, such as wear and the integrity of the adhesive interface, may have induced changes in marginal adaptation over the one year of clinical use.

As Filtek Silorane Restorative System has been conceived by its manufacturer for posterior restorations only, Class I and II lesions were selected for this study. The resulting cavity designs produce high C-factor values, which contribute to higher shrinkage stress. The application technique of the resin composite may also influence the bonding effectiveness.36 In this study, the incremental technique was used in all restorations, as it has been demonstrated to benefit the bond strength of both methacrylate-based37,38 and silorane composites.36

The higher polymerization shrinkage of Filtek Z250 combined with high C-factor may create a more unfavorable environment than is associated with Filtek Silorane, as the silorane composite has been reported to undergo up to 1% volumetric shrinkage,5 according to the manufacturer's information. However, recent research has found Filtek Silorane's volumetric shrinkage to be slightly higher (1.4%)6,10 and close to the 1.7% total volumetric shrinkage determined for Filtek Z250.6 Moreover, the elastic modulus of Filtek Silorane is also higher than that of Filtek Z250, which might be attributed to a more significant influence of the organic matrix on composite stiffness.6 Although the relationship between elastic modulus and polymerization stress is still not well defined, the in vitro study by Boaro and others6 measured a greater polymerization stress for Filtek Silorane than for Filtek Z250, which contradicts the belief that lower polymerization shrinkage is related to lower polymerization stress values, as was originally expected.39 These studies confirm that reduced shrinkage per se does neither guarantee attenuation of stress in restored teeth,10 nor does it improve the interfacial integrity of the restoration,6 which is in line with the findings of previous clinical studies.25,40 The authors of another clinical report41 related to Filtek Silorane analyzed exclusively the marginal adaptation and reported better marginal adaptation for the methacrylate-based resin composite (Ceram.X, Dentsply) compared to that of Filtek Silorane.

Many of the marginal defects detected in the present study appeared to result from the fracture of thin areas of resin composite flash that extended to non-instrumented enamel surfaces adjacent to the cavity margins. Better contouring at polishing should eliminate these areas of marginal flash. Mild self-etch systems have a less stable bonding capacity to enamel, probably because of a shallower etching pattern.42,43 The use of adhesives with a more efficient etching capacity may have reduced the occurrence of such defects, especially in high-stress-bearing areas, because of the improvement of enamel etching.44

The adhesive system that accompanies Filtek Silorane requires separate light-curing of the primer and the bonding, thereby establishing the bonding mechanism to dentin in the first application step, resembling one-step self-etch adhesives. This bonding mechanism uses a form of nano-interaction, typical of ultra-mild self-etch adhesives, which is related to the relatively high pH (2.7) of the respective primer. Mine and others13 observed a tight superficial interaction and very slight inter- and intracrystallite demineralization with subsequent resin infiltration, when bonded to enamel. This nano-interaction bonding mechanism is clinically relevant for a methacryloyloxydecyl dihydrogen phosphate (MDP)-based two-step self-etch adhesive45 and may also occur with the polyalkenoic acid copolymer46 (or Vitrebond™ copolymer) incorporated in the two-step self-etch Silorane System Adhesive used in the present study. Recent in vitro research46,47 found evidence of the Vitrebond carboxylic acid reacting with calcium ions. It has been demonstrated13,47 that the Silorane System Adhesive provides a tight, stable, and water-resistant adhesion to dentin. However, information about its performance when it is bonded to enamel is still scarce.

As mentioned above, the Filtek Silorane Restorative System has been specially designed for posterior restorations, for which the esthetic requisites are not so relevant. Accordingly, the manufacturer only provides four shades. At the six-month and one-year assessments three restorations were rated as Bravo. It is noteworthy that the two Bravo ratings with Filtek Silorane at baseline were caused by the poor esthetic characteristics of the silorane-based resin composite (Figure 3). In fact, evaluators deemed these restorations too yellow and very opaque; thus, their translucency differed from that of tooth structure (Figure 3). Both restorations were also rated Bravo in the subsequent follow-up assessments; therefore, only one restoration showed a real color modification over time. These observations derived from the in vivo analysis are consistent with recent in vitro research demonstrating low translucency and high color stability of silorane-based resin composite compared to those of methacrylate-based resin composites.48,49

Figure 3. . First molar. Occlusal-palatine restoration with the Filtek Silorane Restorative System. Although Filtek Silorane composite displayed a yellowish and opaque appearance in some restorations, the restorations shown were rated Alfa for color match. No staining was detected. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 3. . First molar. Occlusal-palatine restoration with the Filtek Silorane Restorative System. Although Filtek Silorane composite displayed a yellowish and opaque appearance in some restorations, the restorations shown were rated Alfa for color match. No staining was detected. B, baseline; 6M, six-month recall; 1Y, one-year recall.Figure 3. . First molar. Occlusal-palatine restoration with the Filtek Silorane Restorative System. Although Filtek Silorane composite displayed a yellowish and opaque appearance in some restorations, the restorations shown were rated Alfa for color match. No staining was detected. B, baseline; 6M, six-month recall; 1Y, one-year recall.
Figure 3.  First molar. Occlusal-palatine restoration with the Filtek Silorane Restorative System. Although Filtek Silorane composite displayed a yellowish and opaque appearance in some restorations, the restorations shown were rated Alfa for color match. No staining was detected. B, baseline; 6M, six-month recall; 1Y, one-year recall.

Citation: Operative Dentistry 37, 2; 10.2341/11-179-C

CONCLUSIONS

The clinical performance of the Filtek Silorane Restorative System was found acceptable after one year. Additionally, stable adhesion to enamel with self-etch adhesives is still a challenge, as both restorative systems including these products showed a deterioration of their marginal adaptation after one year.

Despite the limitations of this study, the clinical outcomes led to the perception that the Filtek Silorane Restorative System did not provide any remarkable advantage for the evaluated criteria when compared to the other systems, and they reinforced the findings that etch-and-rinse adhesives are still the benchmark when it comes to clinical performance. Further recalls are planned to follow up with regard to the clinical performance of these restorations, as wider differences between the restorative materials might surface at later stages.

Acknowledgments

The authors thank 3M ESPE for the generous donation of the adhesives and resin composites tested. This study is part of a thesis to be submitted in partial fulfilment of the requirements for the PhD degree of author BB.

Conflict of Interest Declaration

The authors of this manuscript certify that they have no proprietary, financial or other personal interest of any nature or kind in any product, service and/or company that is presented in this article except for the following: Dr. Cabrera reports personal/financial interest in 3M ESPE; Dr. Cabrera accepted employment from 3M after this manuscript was accepted by Operative Dentistry.

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Copyright: Operative Dentistry, Inc. 2012
Figure 1. 
Figure 1. 

First molar. Occlusal restoration with Adper Scotchbond SE and Filtek Z250. Staining around this Class I restoration was observed at six-month and one-year evaluations, being rated Charlie (>50% of cavo-surface is affected). Furthermore, the one-year photograph shows that staining has progressed in depth across the adhesive interface. This stain also caused color changes in the resin composite close to the bonded walls. B, baseline; 6M, six-month recall; 1Y, one-year recall.


Figure 2. 
Figure 2. 

First molar. Occlusal restoration with Adper Scotchbond 1 XT and Filtek Z250. This restoration preserved its original aspect after six months and one year. No signs of adhesive deterioration were found. B, baseline; 6M, six-month recall; 1Y, one-year recall.


Figure 3. 
Figure 3. 

First molar. Occlusal-palatine restoration with the Filtek Silorane Restorative System. Although Filtek Silorane composite displayed a yellowish and opaque appearance in some restorations, the restorations shown were rated Alfa for color match. No staining was detected. B, baseline; 6M, six-month recall; 1Y, one-year recall.


Contributor Notes

Bruno Baracco, DDS, professor, Rey Juan Carlos University, Department of Stomatology, Madrid, Spain

Jorge Perdigão, DMD, MS, PhD, University of Minnesota, Restorative Sciences, Minneapolis, MN, USA

Elena Cabrera, DDS, Rey Juan Carlos University, Department of Stomatology, Alcorcón, Spain

Isabel Giráldez, DDS, Rey Juan Carlos University, Department of Stomatology, Alcorcón, Spain

Laura Ceballos, DDS, PhD, Rey Juan Carlos University, Department of Stomatology, Madrid, Spain

Corresponding author: Avda. Atenas s/n, Alcorcón, Madrid 28922, Spain; e-mail: laura.ceballos@urjc.es
Accepted: 06 Sept 2011
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